An alternative, improved method to determine mechanical properties from indentation testing is presented. This method can determine the elastic modulus, yield strength and equi-biaxial residual stress from one simple test. Furthermore, the technique does not require the knowledge of the contact area during indentation, a parameter that is hard to determine for highly elastic material. The evaluation technique is based on finite element analyses, where explicit formulations are established to correlate the parameter groups governing indentation on stressed specimens.
1.
Oliver
, W. C.
, and Pharr
, G. M.
, 1992, “An Improved Technique for Determining Hardness and Elastic-Modulus Using Load and Displacement Sensing Indentation Experiments
,” J. Mater. Res.
0884-2914, 7
, pp. 1564
–1583
.2.
Johnson
, K. L.
, 1985, Contact Mechanics
, Cambridge U.P.
, Cambridge
.3.
Hay
, J. C.
, Bolshakov
, A.
, and Pharr
, G. M.
, 1999, “A Critical Examination of the Fundamental Relations Used in the Analysis of Nanoindentation Data
,” J. Mater. Res.
0884-2914, 14
, pp. 2296
–2305
.4.
Chen
, X.
, Yan
, J.
, and Karlsson
, A. M.
, 2006, “On the Determination of Residual Stress and Mechanical Properties by Indentation
,” Mater. Sci. Eng., A
0921-5093, 416
, pp. 139
–149
.5.
Pharr
, G. M.
, 1998, “Measurement of Mechanical Properties by Ultra-low Load Indentation
,” Mater. Sci. Eng., A
0921-5093, 253
, pp. 151
–159
.6.
Xu
, Z.-H.
, and Li
, X.
, 2005, “Influence of Equi-biaxial Residual Stress on Unloading Behaviour of Nanoindentation
,” Acta Mater.
1359-6454, 53
, pp. 1913
–1919
.7.
Tsui
, T. Y.
, Oliver
, W. C.
, and Pharr
, G. M.
, 1996, “Influences of Stress on the Measurement of Mechanical Properties Using Nanoindentation. 1. Experimental Studies in an Aluminum Alloy
,” J. Mater. Res.
0884-2914, 11
, pp. 752
–759
.8.
Bolshakov
, A.
, Oliver
, W. C.
, and Pharr
, G. M.
, 1996, “Influences of Stress on the Measurment of Mechanical Properties Using Nanoindentation. 2. Finite Element Simulations
,” J. Mater. Res.
0884-2914, 11
, pp. 760
–768
.9.
Suresh
, S.
, and Giannakopoulos
, A. E.
, 1998, “A New Method for Estimating Residual Stresses by Instrumented Sharp Indenter
,” Acta Mater.
1359-6454, 46
, pp. 5755
–5767
.10.
Swadener
, J. G.
, Taljat
, B.
, and Pharr
, G. M.
, 2001, “Measurement of Residual Stress by Load and Depth Sensing Indentation With Spherical Indenters
,” J. Mater. Res.
0884-2914, 16
, pp. 2091
–2102
.11.
Lee
, Y. H.
, and Kwon
, D.
, 2003, “Measurment of Residual-Stress by Nanoindentation on Elastically Strained (100) W
,” Scr. Mater.
1359-6462, 49
, pp. 459
–465
.12.
Lee
, Y. H.
, and Kwon
, D.
, 2004, “Estimation of Biaxial Surface Stress by Instrumented Indentation With Sharp Indenters
,” Acta Mater.
1359-6454, 53
, pp. 1555
–1563
.13.
Carlsson
, S.
, and Larsson
, P. L.
, 2001, “On the Determination of Residual Stress and Strain Fields by Sharp Indentation Testing. Part I: Theoretical and Numerical Analysis
,” Acta Mater.
1359-6454, 49
, pp. 2179
–2191
.14.
Carlsson
, S.
, and Larsson
, P. L.
, 2001, “On the Determination of Residual Stress and Strain Fields by Sharp Indentation Testing. Part II: Experimental Investigation
,” Acta Mater.
1359-6454, 49
, pp. 2193
–2203
.15.
Chen
, X.
, and Vlassak
, J. J.
, 2001, “Numerical Study on the Measurement of Thin Film Mechanical Properties by Means of Nanoindentation
,” J. Mater. Res.
0884-2914, 16
, pp. 2974
–2982
.16.
Mesarovic
, S. D.
, and Fleck
, N. A.
, 1999, “Spherical Indentation of Elastic-Plastic Solids
,” Proc. R. Soc. London, Ser. A
1364-5021, 455
, pp. 2707
–2728
.17.
ABAQUS, 2004, “
ABAQUS 6.5
,” ABAQUS Inc., Pawtucket, RI.18.
Bowden
, F. P.
, and Tabor
, D.
, 1950, The Friction and Lubrications of Solids
, Oxford U.P.
, Oxford
.19.
Cheng
, Y.
, and Cheng
, C.
, 2004, “Scaling, Dimensional Analysis, and Indentation Measurements
,” Mater. Sci. Eng., R.
0927-796X, 44
, pp. 91
–149
.20.
Bucaille
, J.
, Stauss
, S.
, Felder
, E.
, and Michler
, J.
, 2003, “Determination of Plastic Properties of Metals by Instrumented Indentation Using Different Sharp Indenters
,” Acta Mater.
1359-6454, 51
, pp. 1663
–1678
.21.
Wang
, L.
, and Rokhlin
, S.
, 2005, “Universal Scaling Functions for Continuous Stiffness Nanoindentation With Sharp Indenters
,” Int. J. Solids Struct.
0020-7683, 42
, pp. 3807
–3832
.22.
Wei
, G.
, Bhushan
, B.
, and Jacobs
, S.
, 2004, “Nanomechanical Characterization of Multilayered Thin Film Structures for Digital Micromirror Devices
,” Ultramicroscopy
0304-3991, 100
, pp. 375
–389
.23.
Zagrebelny
, A. V.
, and Carter
, C. B.
, 1997, “Indentation of Strained Silicate-Glass Films on Alumina Substrates
,” Scr. Mater.
1359-6462, 37
, pp. 1869
–1875
.24.
Pelletier
, H.
, Krier
, J.
, Cornet
, A.
, and Mille
, P.
, 2000, “Limits of Using Bilinear Stress-Strain Curve for Finite Element Modeling of Nanoindentation Response on Bulk Materials
,” Thin Solid Films
0040-6090, 379
, pp. 147
–155
.25.
Schwarzer
, N.
, and Pharr
, G.
, 2004, “On the Evaluation of Stresses During Nanoindentation With Sharp Indenters
,” Thin Solid Films
0040-6090, 469–70
, pp. 194
–200
.26.
Yan
, J.
, Karlsson
, A. M.
, and Chen
, X.
, 2006, “Determining Plastic Properties of a Bulk Material With Residual Stress by Using Conical Indentation
,” Int. J. Solids Struct.
0020-7683, in press.Copyright © 2007
by American Society of Mechanical Engineers
You do not currently have access to this content.